PARTICLE SIZE AND PARTICLE SHAPE
Laser Light Scattering – Mie and Fraunhofer Theories
PSA – 01 (Formerly 520-00)
Aqueous – dispersion (ISO 13320) using Saturn DigiSizer
USA only
PSA – 02 (Formerly 520-01)
Non-aqueous – based dispersion (ISO 13320) using Saturn DigiSizer
USA only
PSA – 03 (Formerly 520-50)
Dry dispersion (ISO 13320) using Malvern Mastersizer
USA only
PSA – 04 (Formerly 520-51)
Liquid dispersion (ISO 13320) using Malvern Mastersizer
USA only
X – Ray Sedimentation – Stokes‘ Law
PSA- 05 (Formerly 510-00)
Aqueous and non-aqueous based dispersion inorganic materials only (ISO 13317-3) (Requires Density- 01 prior to analysis if skeletal density is not provided
337€
Particle Shape Analysis
SEM – 04 (Formerly 005-81)
Particle shape using an automated microscopy technique
USA only
Nano Particle Size
Physi – 23 (Formerly 005-70)
Average particle size calculated from BET surface area
333€
PSA-10 (Formerly 005-71)
Dynamic light scattering/ photon correlation spectroscopy (ISO 22412)
USA only
Other Particle Size Techniques
PSA-11 (Formerly 005-73)
Particulate count and concentration using the light obscuration technique (USP method <788> and<789>)
USA only
PSA-12 (Formerly 005-74)
Sub-Sieve AutoSizer (ASTM B330-07 , ASTM C721, 150-10070) (Requires density prior to analysis) Air permeability diameter
USA only
PSA-14 (Formerly 010-16)
Dry or wet sieving available/ Ro-Tap apparatus
USA only
PSA-15 (Formerly 010-78)
Particle size of material on filters
USA only
SEM – 03 (Formerly 010-SO)
Particle size using automated microscopy techniques
USA only
Zeta Potential
PSA-16 (Formerly 120 -00)
Zeta potential (ISO 13099-2)
USA only
PSA-17 (Formerly 120-01)
ISO-electric point determination and pH titration
USA only
Mayer – Stowe
PSA-18 (Formerly 942 -09)
Particle size calculation from Mercury intrusion analysis
407€
B.E.T. OR LANGMUIR SURFACE AREA; T-PLOT AREA
Physi – 01 (Formerly 005-01)
Multipoint surface area using nitrogen gas (ISO 9277)
280€
Physi – 02 (Formerly 005-02)
Multipoint surface area using krypton gas (ISO 9277)
323€
Physi – 04 (Formerly 005-10)
Multipoint surface area and STSA using nitrogen gas (ASTM D6556)
375€
PORE VOLUME DISTRIBUTION/PORE SIZE DISTRIBUTION
Pore Size by Gas Adsorption:
Pore size samples may include the following reports as appropriate: BET or Langmuir surface area, BJH mesopore analysis, DFT pore size calculations, single-point total pore volume, and t-Plot micropore volume (ISO 15901-02).
Physi – 10 (Formerly 005-50)
40-point nitrogen adsorption isotherm (20 A to 3000 A)
442€
Physi -12 (Formerly 005-08)
40-pt Nitrogen adsorption and 40-pt desorption isotherm (20 A to 3000 A)
641€
Micropore Pore Size Distribution:
Reports may include H-K, Dubinin, and/or DFT methods for micropore analysis (ISO 15901-3) .
Physi-13 (Formerly 201-03)
High-resolution micropore analysis plus mesopore isotherm (4 A to 3000 A)
1116€
Pore Size by Mercury Intrusion
Report will include calculations of bulk density, skeletal density, porosity, average pore diameters, median pore diameters, and total intrusion volume. Additional summary reports such as tortuo slty, fractal dimension, permeability, and compressibility are available upon request for an additional fee (ISO 15901-01).
MIP – 01 (Formerly 942-03)
Mercury intrusion analysis (pore size range 360 to 0.003 μm)
428€
MIP – 02 (Formerly 942 – 04)
Mercury Intrusion and extrusion analysis (pore size range 360 to 0.003 μm)
481€
MIP -03 (Formerly 942-10)
High-resolution macropore analysis (pore size range 900 to 4 μm)
397€
MIP – 04 (Formerly 942 -11)
High-resolution macropore plus a complete intrusion and extrusion analysis
606€
MIP-05
Reverberi method for pore throat and pore cavity
721€
MIP – 10 (Formerly 942-05)
Advanced Hg calculations
95€
DENSITY
Density- 01 (Formerly 133 – 00)
Skeletal density (Helium or Nitrogen pycnometry) ISO 12154, USP <699>
150€
Density- 02 (Formerly 133 – 01)
Skeletal density at specific temperature
185€
Density – 03 (Formerly 133 – 02)
Open cell content of rigid cellular plastic, foam density (ASTM 06226)
238€
Density- 04 (Formerly 136 – 00)
Envelope density of solid, non-powder samples using the GeoPyc“‚ 1360
185€
Density- 05 (Formerly 136 – 01)
T.A.P.™ (Transverse Axial Pressure) density using the GeoPyc® 1360
USA Only
Density – 07 (Formerly 942 – 07)
Mercury bulk density
319€
Density – 08 (Formerly 010 – 70)
Bulk and Tap density USP <616>
USA Only
Density – 09 (Formerly 010 – 77)
Bulk density only
USA Only
SPECIAL VAPOR SORPTION SERVICES
Physi – 20 (Formerly 005 – 60)
Special CO2 isotherms at O °C
684€
Physi – 21 (Formerly 005 – 60)
Adsorption isotherms at user defined conditions (specialty gases)
1055€
Physi – 22 (Formerly 005 – 61)
High-pressure isotherms using hydrogen, nitrogen, oxygen, methane, or other gases
USA only
Vapor – 01 (Formerly 005 – 63)
Vapor isotherms – Dynamic vapor sorption (DVS) gravimetric analysis
USA only
Vapor – 02 (Formerly 005 – 64)
Vapor isotherms using volumetric technique (ASAP 2020 or 3Flex)
936€
Vapor – 03 (Formerly 005 – 65)
Inverse gas chromatography (surface energy measurement)
USA only
Vapor- 04 (Formerly 005 – 75)
Surface energy heterogeneity profile (BET surface area required)
USA only
CHEMISORPTION
Chemi – 01 (Formerly 201 -10)
Volumetric chemisorption analysis (specify analytical method)
USA only
Chemi – 02 (Formerly 291- 23)
Dynamic or pulse chemisorption analysis (specify analytical method)
879€
Chemi – 03 (Formerly 291- 03)
Pulse chemisorption using liquid vapors (specify analytical method)
986€
Temperature-Programmed Studies
Chemi – 04 (Formerly 291- 01)
Temperature-Programmed Reduction (TPR)
747€
Chemi – 05 (Formerly 291-10)
Temperature-Programmed Desorption (TPD)
747€
Chemi – 06 (Formerly 291- 02)
Temperature-Programmed Oxidation (TPO)
747€
Chemi – 07 (Formerly 291- 06)
Mass spectrometry analysis (must be combined with temperature program study)
USA only
Other Chemisorption Experiments
Chemi – 21 (Formerly 201- SO)
Isosteric heat of adsorption
Call
Chemi – 22 (Formerly 291- 20)
Heat of desorption, first order kinetics
Call
MICROSCOPY
SEM – 01 (Formerly 010 – 40)
SEM images using table-top SEM
USA only
SEM – 02 (Formerly 010 – 41)
Elemental analysis by energy dispersion spectroscopy and SEM Imaging
USA only
POWDER RHEOLOGY
Powder – 01
Complete set of powder testing using the FT4, including dynamic flow properties, bulk powder properties and shear properties. A summary report will be provided.
USA only
Powder – 02
Dynamic flow properties Include basic flowability , aeration test ing and consolidation test ing along with summary report.
USA only
Powder – 03
Bulk powder property testing includes compressibility and permeability testing along with a summary report
USA only
Powder- 04
Shear property testing includes shear cell testing and wall friction testing along with a summary report.
USA only
Powder-05
Individual powder property testing , choose from flowability , aeration, consolidation, compressibility, permeability, shear and wall friction testing. Price Is per test and per sample. No summary report available.
USA only
CAPILLARY FLOW POROMETRY
Filter-01
Scanning porometry of pore sizes down to 30 nm using a POROLUXTM 100/l OONW; 500
USA only
SCIENTIFIC SERVICES
PTA- 01 (Formerly 010 – 00)
Non-standard laboratory analysis
Call
PTA-02 (Formerly 010-10)
Method development services
Call
PTA- 03 (Formerly 010-11)
Method validation services
Call
PTA-04
Method verification or method transfer
Call
PTA- 05 (Formerly 010- 06)
Consulting services and detailed results interpretation
Call
OTHER SERVICES
PTA-06 (Formerly 010-80)
Special sample preparation or storage (glove box or freezer)
USA only
PTA – 10 ( Formerly 005 – 87)
Expert testimony
Call
PTA-13 (Formerly 010-01)
Certificate of analysis
86€
PTA-40 (Formerly 005- 85)
Dynamic void volume – DVVA (ASTM D7854)
USA only
SEM – 03 (Formerly 010 – 50) Call
Contamination or particle identification (outsourced)
Call
MIP-11 (Formerly 950-50)
Volume calibration of AutoPore Mercury penetrometers
323€
VOLUME DISCOUNT SCHEDULE
Volume discounts are based on the number of samples sent in for same test number, not just total number of samples .
6-10 samples
5%
Discount
11-20 samples
10%
Discount
21-40 samples
15%
Discount
More than 40 samples
20%
Dicount
SAMPLE TURNAROUND TIMES
Turnaround times are typical for most samples. Some exclusions do apply.
Normal (Typically within 7 business days)
List Price
Priority (Typically2 to 4 business days)
List Price + 50% surcharge
Rush (Next sample analyzed)
List Price+ 200% surcharge
All orders are subject to Particle Testing Authority terms and conditions (see separate terms and conditions document at www.particletesting.com ). Credit card orders are welcomed .
Unless otherwise requested, samples will be retained for a minimum of 3 months. Samples can be returned at the customer’s expense, provided correct shipping and payment information is received. Sample results will be maintained for a minimum of 5 years. All samples and related customer information is kept confidential.
INSTRUMENT PURCHASE ALLOWANCE
Half the cost of applicable analyses completed within 120 days of instrument purchase may be credited toward instrument purchase. The maximum credit allowed is 4% of the instrument purchase price. Customer must notify Micromeritics of credit due when instrument is ordered.
RETURN SAMPLE FEE
There is a flat fee of 60€ per project for all sample returns. 160€ if samples are considered hazardous. unless an account number is provided. SDS are required for all samples .
Please review the Terms and Conditions
TERMS: Net 30 days … for 45 days add 2%, for 60 days add 4% to the final negotiated price .
For tests available in USA only, please see USA price list and contact the Norcross, GA Laboratory at mas@particletesting.com