SediGraph

Distribución granulométrica de partículas inorgánicas por sedimentación de rayos X

  • 0.1 to 300 µm particle diameter
  • Large (50 mL dispersed) volume for representative sampling of heterogeneous materials
  • Complete particle accounting – including particles outside the direct measurement range
  • Available automation: measure up to 18 samples unattended
  • Conforms to ISO 13317-3, ASTM B761 and Committee C28 on Advanced Ceramics

Visión general

The Micromeritics SediGraph continues to be a prefered standard instrument for particle size analysis in many laboratories throughout the world. Whether in a rugged production environment or a controlled laboratory setting, the SediGraph continues to produce accurate results with superior reliability. Particle size distribution is measured using the sedimentation method. Particle mass is measured directly via X-ray absorption. By measuring the rate at which particles fall under gravity through a liquid having known properties as described by Stokes’ law, the SediGraph determines the equivalent spherical diameter of particles ranging from 0.1 to 300 µm.

The new generation SediGraph III Plus combines this proven technique with new technology to deliver reproducible and highly accurate particle size information, completing most analyses in minutes.

Why SediGraph?

Technology

The SediGraph III Plus determines particle size distributions and statistics, such as D10, D50, and D90, based on direct mass concentration detection. Basic and advanced reporting available at the touch of a button. The SediGraph III Plus can be coupled with an optional MasterTech autosampler for continuous monitoring of a production process and have data pushed to a network or cloud for remote access.

Software

The SediGraph III Plus is equipped with a versatile, easy-to-use user interface that provides all of the convenient features you expect from a Windows-based program. These features include point-and-click menus, customizable reports with your laboratory logo graphic, editable graphs, cut-and-paste graphics and tables, data export features, and more. Custom protocols help plan, launch, and control the analysis and assure that subsequent analyses are all performed in the same manner, regardless of the skill of the operator. You can collect, organize, archive and reduce raw data, and store standardized sample information and analysis conditions for easy access during later applications. Finished reports may be generated to screen, paper, or transferred in a variety of formats to storage devices.

Detailed analysis data for particles ranging from 300 to 0.1 µm are provided automatically by the SediGraph III Plus. Data collected from other particle size analyses ranging from 125,000 to 300 µm can be combined with SediGraph data, enabling effective reporting for particles ranging from 125,000 to 0.1 µm.

In addition to tabular data, different graphical analysis plot types are available including:

  • Cumulative Mass, Area, and Number
  • Settling Velocity Distribution
  • Process Control Charts
  • Log Probability
  • Baseline/Full Scale References
  • Frequency Distribution
  • Difference From Reference
  • Out of Specification
  • Rosin-Rammler
  • Regression Analyses

Plots can be overlaid for comparing the results from different samples or for comparing different plot types from the same sample. This allows you to compare analysis results to a standard. Plots can be rescaled to give you the ability to scrutinize closely your graphical data. A column has been added to the tables and to the x-axis selection in the graphs that reports size in Phi units, where Ф = -log2 (particle diameter in mm). Also, a column selection for settling velocity (cm/s) is available for tables. The x-axis of plots can be scaled in particle size or settling velocity.

Accessories

The MasterTech™ 052 Autosampler

The MasterTech 052 Autosampler provides assurance that samples are prepared and analyzed exactly the same way, every time. The MasterTech is designed to increase throughput, repeatability, and reproducibility while reducing operator involvement. Up to 18 samples can be queued to run sequentially and completely unattended, including automatic stirring or sonication prior to transfer to the analysis system. The SediGraph’s operating software controls the MasterTech, and information about dispersion is stored in the sample file for future reference.

The MasterTech features a powerful ultrasonic probe for sample redispersion. Power to the probe tip is adjustable and the driving circuit is self-tuning for maintaining efficient and consistent sonic energy levels. A front-panel digital readout lets you know when the desired power is reached, and that same power is applied each time the method is repeated. The SediGraph III Plus is designed to accommodate the MasterTech on top of the analytical unit, thus conserving valuable bench space.

Applications

Ceramics

The size range of particles and the distribution of mass in each...

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Metal Powders

By controlling particle size, very specific pore characteristics can be designed into...

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Geological/Soil Science

Grain Size affects the moisture-holding capacity of soil, drainage rate, and the...

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Cosmetics

The appearance, application, and packaging of cosmetics are influenced by the particle...

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Pigments

Particle size alone can affect the tinting strength of a color. As...

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Catalizadores

Particle size affects the catalytic activity of a metal for structure-sensitive catalytic...

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Construction Materials

Particle size of cement affects setting time and strength characteristics of finished...

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Minerals and Inorganic Chemicals

Reactivity of materials is dependent upon exposed surface area and thus particle...

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Abrasives

A properly balanced size distribution of abrasive grains and powders is a...

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Capacidades

Specifications
Particle Diameter Range

0.1 to 300 µm Equivalent Spherical Diameter

Wetted Materials

Stainless steel, Teflon® impregnated anodized aluminum, nickel plated aluminum, nylon, polypropylene, polystyrene, Tygon® and Pharmed® tubing, tungsten carbide, Ertalyte®, Viton®, Buna-n, and epoxy

Sample Size

50 mL of dispersed sample – precise concentration is not required

Suspending Liquids

Any liquid compatible with sample cell materials and not highly absorptive of Xrays (typical liquids are water, glycols, mineral oils, SediSperse®, and alcohols)

Power Requirements

85 to 264 VAC, 47/63 Hz, 450 VA

Temperatura

Ambient +10 to 40 °C, operating; -10 to 55°C, storing or shipping

Humedad

20 to 80% (non-condensing)

Físico

Height: 52 cm (20.5 in.)
Width: 50.5 cm (20 in.)
Depth: 58 cm (23 in.)
Weight: 43 kg (95 lbs)

Las especificaciones facilitadas eran válidas según los documentos disponibles en el momento de su publicación. Estas especificaciones pueden cambiar sin previo aviso y sólo se proporcionan como referencia general.

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SediGraph III 5125

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