AutoPore V

Leading performance for mesoporous and macroporous materials coupled with class-leading operational safety

  • Widest range of measurable pore sizes: from as 3 nm to 1100 µm.
  • High resolution analysis for macroporous and mesoporous materials in both intrusion and extrusion anlayses.
  • New enhancements focus on improving operator safety.
  • Flexible method definition optimizes for speed or resolution as needed.
  • Powerful, customizable reporting system produces actionable measurement outputs.
  • Complies with the ASTM Methods D4284, D4404, and D6761, as well as ISO 15901-1 and USP <267>.

Overview

Class Leading, Proven Performance

The mercury porosimetry analysis technique is based on the intrusion of mercury into a porous structure under stringently controlled pressures. Besides offering speed, accuracy, and a wide measurement range, mercury porosimetry permits you to calculate numerous sample properties such as pore size distributions, total pore volume, total pore surface area, median pore diameter and sample densities (bulk and skeletal).

The AutoPore V Series Mercury Porosimeters can determine a broader pore size distribution more quickly and accurately than other methods. This instrument also features enhanced safety features and offers new data reduction and reporting choices that provide more information about pore geometry and the fluid transport characteristics of your material.

Features

1

Triple Fail Safe - 2
Interlock on Locking Cap

2

Mercury Collection Trays

3

Improved Mercury Funnel Design

4

Mercury Vapor Detection Device

1. Triple Fail Safe - 2 Interlock on Locking Cap

Verifies that capacitance detector is installed on low-pressure port, automatically suspends run, and permits user to check filling of the penetrometer prior to run

2. Mercury Collection Trays

Safe collection of mercury for disposal in the case of compromised penetrometer seals or operator error resulting in broken penetrometers

3. Improved Mercury Funnel Design

Attached screw cap and funnel-shaped opening eliminates mercury contamination and possible drip-spillage associated with separate detached filling funnel. Attached screw cap prevents loose cap and possible vapor release

4. Mercury Vapor Detection Device

Handheld device to check localized mercury vapor levels that exceed defined safety limits. Portable device allows point checks at the instrument or any location within the lab exposed to mercury

Triple Fail Safe - 1 Penetrometer Safety Cap

In case of operator error, this device prevents the penetrometer or rod being released from port unintentionally

Triple Fail Safe - 3 System Pressure Vent on Manifold

Works in concert with Cap Interlock to automatically vent system pressure if above ambient pressure and error condition is detected

Software Control for Fine Powder Samples

Prevents fine powder from accidental aspiration into low-pressure ports during analysis by using intelligent evacuation controlled by sample type

Why AutoPore V?

Technology

Features and Benefits

  • Provides rapid, detailed intrusion and extrusion analysis over a wide range of pore sizes.
  • Nineteen standard penetrometer sizes and configurations allow analysis of a wide variety of sample sizes and shapes.
  • New safety enhances set a new benchmark in operator safety.
  • Scanning and equilibration modes of operation allow for rapid or more detailed analyses, respectively.
  • MicroActive software allows for rapid modification of reporting ranges.
  • Includes user-defined advanced reporting capabilities using Python scripts

Software

complete your workflow

Accessories

Mercury QuikVac
An excellent low-cost method for quickly containing mercury spills
Penetrometer Rack
Safely store and transport penetrometers to prevent breakage and unnecessary replacement.

Penetrometers

Partial List
Model#SizeStem VolumeMediumTypical Use
0115 cc0.392Solidrefractories, low-porosity solid rocks/cores, low porosity solid polymers
0215 cc0.392Powderlow-porosity powders, gravel, irregular rock shapes
0315 cc1.131Solidmedium-porosity rocks/cores, solid materials
0415 cc1.131Powdermedium-porosity rocks, solid materials, fumed silica
075 cc0.392Solidpaper, flexible polymer/membrane sheets, pharma tablets
085 cc0.392Powdersilicates, catalysts, powders (general use), pharma powders
095 cc1.131Solidmedium/high-porosity sheet-form materials (paper, polymer, etc.), pharma tablets
105 cc1.131Powdersilica-alumina, silicates, zeolites, catalysts, powders (general use), pharma powders
143 cc0.412Powderpowders (general use), materials with low quantity available
2415 cc3.263Solidhigh-porosity rock/cores, low-density/high-porosity foams
2515 cc4.185Solidhigh-porosity material with large volume

Applications

Pharmaceuticals

Porosity and surface area play major roles in the purification, processing, blending,...

+

Ceramics

Pore area and porosity affect the curing and bonding of greenware and...

+

Adsorbents

Knowledge of pore area, total pore volume, and pore size distribution is...

+

Catalyst

The active surface area and pore structure of catalysts influence production rates....

+

Aerospace

Surface area and porosity of heat shields and insulating materials affect weight...

+

Fuel Cells

Fuel cell electrodes require controlled porosity with high surface area to produce...

+

Geoscience

Porosity is important in groundwater hydrology and petroleum exploration because it relates...

+

Filtration

Pore size, pore volume, pore shape, and pore tortuosity are of interest...

+

Construction Materials

Diffusion, permeability, and capillary flow play important roles in the degradation processes...

+

Paper

The porosity of print media coating is important in offset printing where...

+

Medical Implants

Surface area and porosity of heat shields and insulating materials affect weight...

+

Capabilities

Specifications
Low Pressure (all models) High Pressure
Measurement 0.2 to 50 psia (345 kPa) 9600/9605: From atmospheric pressure to 33,000 psia
9610/9620: From atmospheric pressure to 60,000 psia
Pore Diameter Range 1100* to 3.6 µm (*calculated with initial filling pressure of 0.2 psia) 9600/9605: 6 to 0.005 µm
9610/9620: 6 to 0.003 µm
Resolution 0.00025 psia 9600/9605: 0.165 psia from 3,300 psia to 33,000 psia
9610/9620: 0.03 psia from atmospheric pressure to 60,000 psia
Transducer Accuracy (transducer manufacturer’s specifications) +/- 1% of full scale +/-0.1% of full scale
Transducer Hysteresis - 0.05% of full scale
Servo Control Precision 1% of target, min 0.05 psia, no overshoot 0.5% of target, min 5 psia, no overshoot
Intrusion Resolution Better than 0.1 all
Intrusion Accuracy +/- 1% of maximum penetrometer stem volume
Gas Nitrogen or other clean, dry gas at 50 psig (345 kPa)
Electrical
Low Pressure (all models) High Pressure
Measurement 0.2 to 50 psia (345 kPa) 9600/9605: From atmospheric pressure to 33,000 psia
9610/9620: From atmospheric pressure to 60,000 psia
Pore Diameter Range 1100* to 3.6 µm (*calculated with initial filling pressure of 0.2 psia) 9600/9605: 6 to 0.005 µm
9610/9620: 6 to 0.003 µm
Resolution 0.00025 psia 9600/9605: 0.165 psia from 3,300 psia to 33,000 psia
9610/9620: 0.03 psia from atmospheric pressure to 60,000 psia
Physical
Low Pressure (all models) High Pressure
Measurement 0.2 to 50 psia (345 kPa) 9600/9605: From atmospheric pressure to 33,000 psia
9610/9620: From atmospheric pressure to 60,000 psia
Pore Diameter Range 1100* to 3.6 µm (*calculated with initial filling pressure of 0.2 psia) 9600/9605: 6 to 0.005 µm
9610/9620: 6 to 0.003 µm
Resolution 0.00025 psia 9600/9605: 0.165 psia from 3,300 psia to 33,000 psia
9610/9620: 0.03 psia from atmospheric pressure to 60,000 psia
Transducer Accuracy (transducer manufacturer’s specifications) +/- 1% of full scale +/-0.1% of full scale

Provided specifications were valid as taken from available documents at time of publication. These specifications may change without notice and are only provided as a general reference

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AutoPore V 9600

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