Using Temperature Programed Analysis for Acid Site Characterization of Solid Acids

September 8, 2021

Visión general

Zeolites are microporous aluminosilicates that are commonly used as catalysts and adsorbents in many applications. Acid site characterization of a zeolite is crucial to gauge and optimize for a wide variety of different catalytic activities. In this case study, the effect of different SiO2/Al2O3 ratios on acidity of ZSM-5 and the effect of heat on Beta Zeolite were explored using the Ammonia Temperature Programmed Desorption. This technique on the AutoChem 2930 provides a simple and reproducible mean to qualitatively analyze solid acids. 

Speaker

Pearl Kim

Pearl Kim

Applications Scientist, Micromeritics Instrument Corporation

Pearl received her BS degrees in chemistry and biochemistry at the University of Georgia. Her undergraduate research involved spectroscopic studies of purified carbon nanotubes with emphasis on UV-vis and Raman spectroscopy and the X-ray protein crystallography with a focus on crystallizing and finishing a Glutathione Reductase mutant structure. She joined Micromeritics in 2017 as a lab analyst, managing physisorption and chemisorption analyses in the PTA lab for a couple years. She joined the applications team in 2020, specializing in physisorption.

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